Question

3. Describe how you would purify p-nitrobenzoic acid from a mixture of 9.0g of p-nitrobenzoic acid...

3. Describe how you would purify p-nitrobenzoic acid from a mixture of 9.0g of p-nitrobenzoic acid and 2.0g of o-nitrobenzoic acid using recrystallization. Tell what solvent you would use and how the components would be separated

Homework Answers

Answer #1

p-nitrobenzoic acid (4-nitrobenzoic acid) having lower melting point than o-nitrobenzoic acid (2-nitrobenzoic acid).

M.P of p-nitrobenzoic acid is 124 oC

M.P. of o-nitrobenzoic acid is 146-148 oC.

Following methods are used for recrysatllization.

Know the answer?
Your Answer:

Post as a guest

Your Name:

What's your source?

Earn Coins

Coins can be redeemed for fabulous gifts.

Not the answer you're looking for?
Ask your own homework help question
Similar Questions
For questions 7 and 8, imagine that we dissolve a mixture of the compounds (3-nitrobenzoic acid,...
For questions 7 and 8, imagine that we dissolve a mixture of the compounds (3-nitrobenzoic acid, 2-naphthol, and 1,4-dimethoxybenzene) in diethyl ether. We then add aqueous sodium hydroxide into the mixture and place the solution into a column. 7. Which layer will elute first? A. Aqueous B. Organic C. Other (Specify) _________________________ 8. Which compounds (if any) would you expect to find in the first layer to elute from the column? (Circle all that apply) A. 3-nitrobenzoic acid B. 2-naphthol...
How would you purify the following compounds (explain what method and solvent you would use). Assume...
How would you purify the following compounds (explain what method and solvent you would use). Assume the contaminant comprises only a small percentage of the mixture. A) decanoic acid contaminated with biphenyl B) Biphenyl contaminated with fluorene C) Fluorene contaminated with ethyl-4-aminobenzoate
Summarize how you would could purify benzhydrol using recrystallization in hexane
Summarize how you would could purify benzhydrol using recrystallization in hexane
Describe how you could seperate and purify compound A from a mixture of two neutral compounds...
Describe how you could seperate and purify compound A from a mixture of two neutral compounds (A and B) when A comprises 95 percent of the total and B the other 5 percent of the total. Assume that A and B have similar polarities
Propose in detail how would you separate and purify a mixture of acetone and toluene. Give...
Propose in detail how would you separate and purify a mixture of acetone and toluene. Give detailed descriptions.
Show the steps for how to isolate 4-aminoacetophenome and benzoic acid from a solid mixture of...
Show the steps for how to isolate 4-aminoacetophenome and benzoic acid from a solid mixture of 4-aminoacetophenome, benzoic acid, and 1,4 - dibromobenzene using acid/base chemistry and recrystallization.
How would you separate a mixture of m-toluic acid and 3-aminoacetophenone using extraction technique?
How would you separate a mixture of m-toluic acid and 3-aminoacetophenone using extraction technique?
If you add HCL to 2-nitrobenzoic acid what are the products that come from that extraction?
If you add HCL to 2-nitrobenzoic acid what are the products that come from that extraction?
PREPARATION OF BENZOCAINE 1. A student wants to prepare benzocaine by oxidizing p-nitrotoluene to p-nitrobenzoic acid,...
PREPARATION OF BENZOCAINE 1. A student wants to prepare benzocaine by oxidizing p-nitrotoluene to p-nitrobenzoic acid, followed by esterification with ethanol and acid and then reducing the nitro group. Do you think the student can prepare benzocaine using this prcodure? Explain your answer. 2. Write the full balanced equations for all three reactions that occur when the saturated sodium bicarbonate solution is added to the cooled reaction mixture. 3. Why it is important to maintain the pH in step #...
If you were to carry out a column chromatography purification for a mixture of benzoic acid...
If you were to carry out a column chromatography purification for a mixture of benzoic acid and naphthalene, what type of solid phase would you use and what type of solvent would you select as an eluting solvent?