Question

Experiment Organic Chemistry 1 - When should you use extraction? - What are the four steps...

Experiment Organic Chemistry 1

- When should you use extraction?

- What are the four steps of extraction? What is the purpose of each step?

(We did extraction of caffeine, but question applies to any)

Homework Answers

Answer #1

Extraction process is a separation technique which is use to separate a desired compound from its matrix.

There are two types of extraction -

1. Liquid-liquid extraction - this uses two I'm miscible liquid to separate a compound which is soluble in one liquid and not in the other.

2. Solid phase extraction - this uses various chemical reaction to extract the compound.

The steps involved in the extraction usually depends on the nature of the compound that you have chosen.

Usually, the compound is extracted with a suitable solvent, then is dried using an anhydrous salt and finally the solvent is evaporated.

Know the answer?
Your Answer:

Post as a guest

Your Name:

What's your source?

Earn Coins

Coins can be redeemed for fabulous gifts.

Not the answer you're looking for?
Ask your own homework help question
Similar Questions
Organic Chemistry Question This question is about an extraction experiment with the compounds biphenyl and 2-chlorobenzoic...
Organic Chemistry Question This question is about an extraction experiment with the compounds biphenyl and 2-chlorobenzoic acid. A student, when conducting this experiment overlooked the instruction "Repeat steps 2 and 3 above two more times with fresh 2 mL portions of sodium bicarbonate solution." Upon conducting TLC analysis, this student found that the final isolated biphenyl was contaminated with some 2-chlorobenzoic acid. Explain, on a molecular level, how and why this student's error led to poor separation. Be specific.
Organic chemistry extraction lab question: Given a mixture of water and an organic solvent which is...
Organic chemistry extraction lab question: Given a mixture of water and an organic solvent which is immisxible with water, we have to determine which layer contains the organic solvent. Why can you not always accurately determine the position of the layer by simply checking the density of water and the organic compound?
For Organic chemistry lab: Distillation: 1. If the heat source in a distillation is a heating...
For Organic chemistry lab: Distillation: 1. If the heat source in a distillation is a heating mantle, why should it be set in a holder so it isn’t resting on the bench top? Would a stirring hot plate have to be held above the bench top? Why must the distilling flask be clamped so it cannot fall? Imagine some problem occurring that requires you to immediately remove the heat from the distilling flask. Think about this, then go back to...
In an Organic Chemistry Lab we were doing the experiment for the preperation of Adipic Acid....
In an Organic Chemistry Lab we were doing the experiment for the preperation of Adipic Acid. We mixed 50mL of H2O, cyclohexene (2mL, density = 0.81 g/cm3), and potassium permanganate (6g). We got 1.19g of Adipic Acid. How do I figure out percent yield and percent error? Please show all of the steps, work, and answers. Thank you
These are grinard experiment questions from organic chemistry lab 1) why is it ao critical to...
These are grinard experiment questions from organic chemistry lab 1) why is it ao critical to the Grinard formation that the diethyl ether solvent be from a freshly-opened can of anhydrous ether? 2) What is the purpose of mechanically-abrading the surface of the Mg pieces prior to use? 3) Work up the magnesium alkoxide product specifies adding cold 1.0M H2SO4 to the crude reaction mixture. Do you think other acids might be used instead of sulfiric for the operation? Why...
1. why must the organic solvent be separated by extraction be insoluble in water. 2. what...
1. why must the organic solvent be separated by extraction be insoluble in water. 2. what is the purpose of washing with water after extraction with a reaction solvent? 3. what is the purpose of using a tared test tube?
1.       Why is the Grignard Reaction so important in Organic Chemistry? 2.       What is the purpose of the...
1.       Why is the Grignard Reaction so important in Organic Chemistry? 2.       What is the purpose of the formation of the Grignard Reagent? 3.       What is the most crucial step during the preparation of the Grignard Reagent? 4.       The end product of a Grignard Reaction is an alcohol. Will it make a difference on the structure of the product if you add a ketone or an aldehyde?
Organic Chemictry Lab Post Lab Questions (Acid-Base Extraction) 1.) In this experiment, if the carboxylic acid...
Organic Chemictry Lab Post Lab Questions (Acid-Base Extraction) 1.) In this experiment, if the carboxylic acid is benzoic acid, how many moles of benzoic acid are present (assume an equal portion of each component)? How many moles of sodium bicarbonate are contained in 1 mL of a saturated aqueous sodium bicarbonate. Is the amount of sodium bicarbonate sufficient to react with all of the benzoic acid? 2.) To isolate the benzoic acid from the bicarbonate solution, the bicarbonate solution is...
So I did a experiment on extraction of caffeine. Here is the question, If your goal...
So I did a experiment on extraction of caffeine. Here is the question, If your goal was to isolate as much caffeine from the aqueous layer as poassible, which of the two methods used in this lab would you use and why? We had 2 methods, first method was using 60 mL of CH2Cl2 to extract second method was using 20 mL of CH2Cl2 three times to extract (60 mL total). Now I know that the second method is better,...
Hi, In organic chemistry Column Chromatography lab experiment there was a question saying What may happen...
Hi, In organic chemistry Column Chromatography lab experiment there was a question saying What may happen if the level of the developing solvent is allowed to fall below the sand layer? What would be the correct answer for it? thanks