Question

For a Diels-Alder Reaction laboratory experiment for Organich Chemistry class. If the hydrolysis to the diacid...

For a Diels-Alder Reaction laboratory experiment for Organich Chemistry class. If the hydrolysis to the diacid is not complete, how could you seperate the desired diacid from the hydrolyzed anhydride by extraction?

Science   Chemistry   
0 0
Add a commentTranscribed image text
Next >

Homework Answers

Answer #1

The diacid can be made to react with a strong base inorder to convert it to the ionic form i.e the dicarboxylate ion which is soluble in water. Now you have two layers, one is an aqueous layer containing the dicarboxylate ion the other an organic layer with the unreacted anhydride. The aqueous layer can be separated using a funnel and the contents can be made to react with a strong acid like HCl. The dicarboxylate ion will react with HCl forming the dicarbxylic acid which being insoluble in aqueous medium will then precipitate out and can be filtered.

0 0
Know the answer?
Your Answer:

Post as a guest

Your Name:

What's your source?

Earn Coins

Coins can be redeemed for fabulous gifts.

Log In

Sign Up

Not the answer you're looking for?
Ask your own homework help question
Similar Questions
In a Diels Alder Reaction, if you had a mixture of the anhydride and the diacid...
In a Diels Alder Reaction, if you had a mixture of the anhydride and the diacid and you were going to use either aqueous acid or aqueous base to separate the 2 compounds, which aqueous solution would you use and why?
Diels Alders Reaction While performing the Diels-Alder reaction between cyclopentadiene and maleic anhydride: (a) Why do...
Diels Alders Reaction While performing the Diels-Alder reaction between cyclopentadiene and maleic anhydride: (a) Why do you have to crack the diene? Draw the reaction that occurs during the cracking process   
Would you expect a Diels-Alder reaction between maleic anhydride and naphthalene to require more or less...
Would you expect a Diels-Alder reaction between maleic anhydride and naphthalene to require more or less harsh conditions than the reaction performed with anthracene? Justify your answer.
The Diels-Alder reaction is one of the most useful in organic chemistry because it allows for...
The Diels-Alder reaction is one of the most useful in organic chemistry because it allows for the formation of rings: The reactor initially has only the diene and the dienophile. The product stream has 55 mole% of the ring and 17 mole% of diene. Calculate the fractional conversion of the limiting reactant and the percentage by which the other reactant is in excess. If we assume that we can do this reaction continuously, pick a basis for the feed and...
How can you tell if Diels- Alder reaction has gone all the way to completion or...
How can you tell if Diels- Alder reaction has gone all the way to completion or not?
Hydrolysis of; 3-methyl-4-cyclohexene-1,2-dicarboxylic anhydride to form a diacid. 1) Could someone please show me the reaction...
Hydrolysis of; 3-methyl-4-cyclohexene-1,2-dicarboxylic anhydride to form a diacid. 1) Could someone please show me the reaction mechanism of Maleic Anhydride, picric acid and piperylene. 2) If you can please also include FMOs and correlation diagrams. 3) Would you know which isomer if piperylene would be more reactive? Trans or Cis? Thankyou.
Chemistry Experiment: Scenario: Your group is working as analytical chemistry interns with the MSU Office of...
Chemistry Experiment: Scenario: Your group is working as analytical chemistry interns with the MSU Office of Environmental Health and Safety (EHS). EHS is responsible for the collection and disposal of all chemical waste on campus. Today, an unidentified white compound was discovered in one of the teaching labs, and your team has been called in to assist with the identification of the compound. Since your team is responsible for safe disposal of the compound, you will also need to determine...
Tuskegee experiment. Most people's initial reaction to the Tuskegee experiment is to ask how it could...
Tuskegee experiment. Most people's initial reaction to the Tuskegee experiment is to ask how it could have happened? What do you think? Given today’s laws of informed consent, could it happen again? Why do you feel that way? How does the Tuskegee study differ from today’s research studies for HIV and AIDS?
We performed a bromination of trans-stilbene in lab (A green chemistry experiment). Suppose that you perform...
We performed a bromination of trans-stilbene in lab (A green chemistry experiment). Suppose that you perform the same reaction under different conditions (in which a different mechanism operates), and you end up with a product that is a mixture of (R,S), (R,R), and (S,S). Which purification technique could be used to isolate the (R,S) compound from the other two stereoisomers? Explain why this technique would be successful. Why can the (R,S) isomer be separated from the other two? Explain your...
1A. The product from your reaction has a sharp melting point, indication that it is either...
1A. The product from your reaction has a sharp melting point, indication that it is either meso-hydrobenzoin or a racemic mixture of the (1R, 2R) and (1S, 2S) enantiomers. Why is it not possible that your product is either the (1R, 2R) or the (1S, 2S) pure enantiomer? 1B. What is the enantiomeric excess (ee) of a racemic mixture of enantiomers? 1C. If the racemic mixture of the hydrobenzoins were formed in the reaction of benzil with sodium borohydride, describe...
ADVERTISEMENT
Need Online Homework Help?

Get Answers For Free
Most questions answered within 1 hours.

Ask a Question
ADVERTISEMENT