In the synthesis of tris(ethylenediamine)nickel (II) chloride dihydrate lab, Give me a good paragraph about this process.. If someone could help me out it would be heavily appreciated.
Synthesis of Tris(ethylenediamine)nickel (II) Chloride
Dihydrate:
Form the Complex Ion:: In a 125-mL
Erlenmeyer flask, dissolve 6 g of nickel(II) chloride hexahydrate
in 10 mL of warm deionized water. Cool the mixture in an ice bath.
In a fume hood, slowly add 10 mL ethylenediamine.
Precipitate the Complex Ion: Cool the
mixture in an ice bath. Cool 15 mL of 95% ethanol to ice bath
temperature and then slowly add it to the solution. Allow the
mixture to settle for complete precipitation of the lavender
product. The supernatant should be nearly colorless.
Isolate the Product: Premeasure the mass
of a piece of filter paper, fitted for a Buchner funnel. Vacuum
filter the product; wash with two 5-mL volumes of cold 95% ethanol
and 5 mL of acetone. Air dry the product and filter paper on a
watchglass. Determine the mass of the filter paper and desire
product
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