Question

In the synthesis of tris(ethylenediamine)nickel (II) chloride dihydrate lab, Give me a good paragraph about this...

In the synthesis of tris(ethylenediamine)nickel (II) chloride dihydrate lab, Give me a good paragraph about this process.. If someone could help me out it would be heavily appreciated.

Homework Answers

Answer #1

Synthesis of Tris(ethylenediamine)nickel (II) Chloride Dihydrate:
Form the Complex Ion:: In a 125-mL Erlenmeyer flask, dissolve 6 g of nickel(II) chloride hexahydrate in 10 mL of warm deionized water. Cool the mixture in an ice bath. In a fume hood, slowly add 10 mL ethylenediamine.
Precipitate the Complex Ion: Cool the mixture in an ice bath. Cool 15 mL of 95% ethanol to ice bath temperature and then slowly add it to the solution. Allow the mixture to settle for complete precipitation of the lavender product. The supernatant should be nearly colorless.
Isolate the Product: Premeasure the mass of a piece of filter paper, fitted for a Buchner funnel. Vacuum filter the product; wash with two 5-mL volumes of cold 95% ethanol and 5 mL of acetone. Air dry the product and filter paper on a watchglass. Determine the mass of the filter paper and desire product

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