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Briefly explain how you would "extract the aqueous layer two times with 5-mL portions of methylene...

Briefly explain how you would "extract the aqueous layer two times with 5-mL portions of methylene chloride."

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Answer #1

Liquid-liquid extraction

Take your aqueous reaction mixture (or aqueous layer containing the compound to be extracted) in a separatory funnel.

Add 5 ml portion of methylene chloride to it. Shake vigorously, and then let it stand for while so that the layers gets separated.

Remove the lower methylnene chloride layer.

Agan add 5 ml of methylene chloride and repeat the process.

Combine the two organic layers and this layer now has compound extracted from aqueous layer into it.

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